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  • Help with Bruker TOPAS for quantitative analysis?
    I am trying to do quantitative analysis using Bruker TOPAS, I followed the following steps:
  • DIFFRACplus TOPAS - UC
    Table 1-2 details step by step procedures provided for most common tasks from single line fitting up to structure determination using selected examples
  • TOPAS - Bruker
    amorphous materials may be quantified as a single group, by spiking the mixture with an internal standard This, however, can only give the total abundance of all compounds without known crystal structure - individual phase amounts are not accessible The TOPAS implementation of PONKCS represents an extremely successfull solution to this problem:
  • PPXRD-13 Workshop Quantitative Phase Analysis by XRPD Bad Herrenalb . . .
    • Mathematical basis of quantitative phase analysis (QPA) is well established Methods for QPA – are mature, extensively covered in literature, and enabled in many software packages – are the same for QPA of crystalline and amorphous content • Amorphous content can be difficult to quantify
  • Analysing the amorphous quantity in internal standards for a more . . .
    Assume a three-phase sample 50% phase A, 30% phase B, 20% amorphous If you add 30% of a 99% crystalline internal standard and do the analysis assuming it is 100% crystalline, you results will come out as 50 5%, 30 3% and 19 2%, which is well within what I consider the precision of normal QPA to be
  • Analysing phase fraction changes using TOPAS - LightForm Wiki
    For two-phase materials, first start with only alpha-phase and refine the parameters, then tick use the beta phase cif and to improve the fit to the second phase Untick crystal size steps (switch off)
  • Bruker XRD TOPAS Quick Start Guide - Laboratory Manuals, Guides, and . . .
    This guide is a quick introduction to the DIFFRAC TOPAS software and how to use the program for profile fitting and Reitveld Refinements For detailed information and an in-depth guide refer to DIFFRAC TOPAS User Guide Technical Reference available in hard copy in the XRD lab or online in Cumulus
  • Percent crystallinity EVA and TOPAS. ppt - ResearchGate
    Both the crystalline and amorphous phase scattering should now be mostly simulated Highlight the Miscellaneous item in the list and click the “Percent Crystallinity” button Choose the peaks





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